Facsimile · p. 379
APPENDIX V. 369 d. Silicic acid.
e. Phosphoric acid.
/. Arsenic, a trace.
The quantitative examination was carried on in the same manner as in the case of sample Xo. 1.
1. Estimation of the Water.
4-527 grm. of ore dried at 110° C. lost 0-065 water = 1-435 % Further heated to a red heat there was a further loss of weight of 0-465 grm 10-271% 2. Estimation of the insohibh x>arts, 2-931 grm. of ore gave 0-5025 grm. insoluble matter 17-144 % 4-7435 grm. of ore gave 0-82108 grm. insoluble matter 17-309% Mean .. .. 17-226% From this 0-82108 grm. of residue, 0-16658 grm. was present as combined silicic acid, or 3-511 % of ore ; that is to say, silicic acid was present in the state of quartz 17-226 - 3-511 = 13-715 %.
3. Estimation of the Pron.
2-931 grm. of ore dissolved, the solution made up to 500""" ; 5Qccm q£ jg solution (B) estimated with a solution of permanganate of potassium, as in No. 1. 21-0""" permanganate of potassium solution was used. This test was tried three times. The result = 0-206388 grm. of oxide of iron, Ye O3, or 70-412 % oxide of iron.
4. Estimation of Phosphoric Acid.
4-7435 grm. of ore gave 0-028765 grm. of phosphate of magnesium, Mg2 P2 0„ corresponding to 0-0184 grm. Pg O5 = 0-39 % phosphoric acid.
VOL. II. 2 B